Eds testing laboratories in Chelmsford? Energy Dispersive Spectroscopy (EDS) identifies the elements present in a sample by analyzing the X-rays generated by the electron beam of the Scanning Electron Microscope (SEM), making it an indispensable tool. Since X-rays are only generated from the area of the surface excited by the small electron beam, spectra of individual areas or particles can be obtained. Spectral information can therefore be generated for an entire field of view by scanning the beam, providing an elemental map. With the high count rate and excellent signal to noise ratio of our advanced QDD EDS detectors, high resolution data sets are collected and analyzed in minutes, rather than days. This elemental mapping technique allows our clients to immediately visualize the chemical landscape in their samples. Additionally, since the entire spectra is stored for each pixel, areas of interest that are identified later can be examined in detail, without ever having to re-image the sample. Other labs can’t touch the quality and visual impact of the elemental maps we produce here at MicroVision Labs.
As indicated in the FTIR spectral comparison below, the suspect material showed a near perfect match for acetylsalicylic acid. Additionally, there was a small amount of dibasic phosphate present. It was determined that the material was likely acetylsalicylic acid with a phosphate binder – an aspirin. Therefore, from this analysis the suspect material in the bottle was likely a household aspirin tablet, broken apart and separated by the water. In order to confirm the identification, a few aspirin tablets from several common manufacturers were obtained, roughly ground, and soaked to allow for comparison. The optical morphology of the crystals, size range of the particles, association with the phosphate and FTIR spectrum all were consistent with the original suspect material. A report detailing the methods and findings in full narrative form was rendered to the client.
Scanning electron microscopy with energy dispersive xray spectroscopy (SEM-EDS) was used to identify the particles. The SEM showed an elevated concentration of iron and iron oxide in the impacted areas. The backscatter electron (BSE) image which correlates brightness in the image with atomic density, highlighted the iron particles that were embedded in the tile and the EDS spectrum confirms the PLM Image chemical composition of these higher density particles.
What if I want a service not listed in your services list? At MicroVision Labs the list of services which we provide to our clients is constantly growing. So if you don’t see what you are looking for give us a call or use the Contact Us tab. Also don’t forget to check our Additional Services Page to see if it might be listed there. Can you identify a contamination or unknown for us? Yes, we call that an Unknown Material ID and we routinely work on that kind of project. We have a number of individual tests designed to classify unknown materials. When combined with our extensive suite of equipment, these tests allow us to identify virtually any material. Give us a call and talk to one of our knowledgeable staff for more information. Read extra info on eds testing.
A client responsible for maintaining the facilities in a public school district called with concerns of a possible mold problem. Areas with high foot traffic, especially those where students tracked water in, were showing dark black spots in the floor tiles. Aggressive cleaning and buffing of the floor would remove the problem for a while, but after several few weeks, the problem resurfaced. The facilities management staff was convinced it was mold related, but sending samples, swabs, and air grabs to a mold lab for culturing showed no sign of fungal structures on the tiles.
MicroVision Laboratories, Inc. has been providing businesses, consultants and other testing laboratories with expert microscopy and analytical services since 2003. Our client base covers a broad spectrum of industries including semi-conductors, aerospace, electronics, biomedical, ceramics, optics, pharmaceuticals, mineralogy, metallurgy, thin films, environmental, membranes filtration and industrial hygiene. Discover even more details at https://microvisionlabs.com/.